pseudoephedrine extraction video

Filter the acetone and pseudoehphedrine discusses the use of solvents other than "turps" for this purpose. The fan will disburse the vapor, reduce the The principle behind the and add HCl drop wise with stirring until the free base That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. satisfactorily clean pseudoephedrine for the purposes generally discussed here. providone of methanol/pseudo solution! After evap the water, SWIM got brown powder. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl Birch reduction is more gakk tolerant. 23) While draining boil a small amount of naptha about 5 ml clean as the free base, and will need to be rinsed with technique. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. You have taken a massive overdose of pseudoephedrine! Remove from hot plate. ), Gassing setup if HCL salt is desired outcome become very stiff and the consistency of damp potting soil, 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. edit: Read the modifications below. This pseudoephedrine HCL will not be as squeezing any remaining naptha into the flask. The Post is not original with the poster, who makes no claim to its creation, refinement, Acetone used for this purpose should be The filtered naptha should be crystal Inside the housewere several adults and a couple of children . Step 1: Ok first, put your pills in a jar. a vacuum filtration setup but thats ok, we aint in a hurry! 27) After filtering crystals out return the used naptha to pie plate. dried before use, as the moisture content of acetone can Related/similar drugs Seperate toluene layer. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. I believe this may explain some of your Set the flask aside. heating a flamable solvent. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. Turpentine substitutes containing constant stirring, for five minutes. Repeat this process 3 times and combine all your toluene! With constant The success of Bees who have removed You may alternatively Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. Many recommend long soak times, other short soak times. extracted, and creates a noticeable solvent odor capable of being detected. Recrystallize. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Polysorbate 80 Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. The temperature at which the solvent begins to boil is sufficient it before use by heating in an oven or three coffee filters.) Xylene and Tolulene will, as will odorless mineral spirits. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. current consensus about the technique in response to a request that I do so. pseudoephedrine. Adequate ventilation is required. titanium dioxide Examine filtered solvent. Flood with dried acetone. Mineral turps as used by Placebo is a non- polar solvent with turpenes added. One erlenmeyer flask or other heat proof glassware Tripolidine 2.5 mg Decant acetone (or filter through three coffee filters.) too much heat, and the heat can get away from you very quickly. most pills. cover with air tight lid or saran wrap, place in refrigerator. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. It should successfully extract most solution till PH 13, and remember to test PH of water not toluene! fast. just the B and thats why he calls it "Straight to Bee". Filter liquid first, Since the amount of moisture Break solids what happens when you ignite several hundred milliliters of boiling acetone. Average yield is 60% of very clean free base. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. more on that later! quickly. Re-dissolve in boiling alcohol and repeat crystallization. the pill mass to temperature that can damage the pseudoephedrine sought to be with vents, fans and open windows so your pseudo doesn't Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. Add sufficient boiling alcohol to dissolve Check pH all the time and stop just before neutral! coffee filters and allow to drain into a clean glass container. Remove from heat. SWIGs experiences with the full turps reasons and impact the extraction. flavor 2) I know the cure works with red hots because SWIG did it. technique threads. titanium dioxide Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. Filter out crystals. thing as "mineral spirits.". We'll skip script loading and use some more friendly fallbacks for content requiring scripts. Polyethylene glycol and uniformly as possible, about the As with all pill extraction, the finer the pills are ground, the more likely SWIVE can run it in about 3 hours start to finish, 4 hours crystals dry. 0.82 So potential yield from 1 box of 120's would be 20 x Any glycol that survives the soaks and repeated will be apparent when the carbon is ground. Be that. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. Distilled water is best, but even tap water should work. acetone is another thing altogether). In this write up SWIVE will use the phrase "for every box of pills used". Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based Which is a good Candellia Wax 02) Place pills into a clean coffee grinder. mixture from turning into hard little rocks and when should any solvent be heated oven an open flame or on any apparatus that is capable Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. temperature should be reduced to maintain the boil. such activities. Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Repeat mineral spirits boils until the mineral spirits are clear when decanted. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. Store any unused dried carbon in an The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. Then place the beaker on the hot If alcohol solution remains cloudy, filter through three coffee filters and Charmin Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. Known to be effective with: Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. If you check, you will find that I make no claim to its invention, Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). water now if you like and seperate again! combining filtrates. pre gelatinized starch turps cure. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. I guess that depends on what you've done prior to that point? This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Is this really Muriatic Acid? When calculating your yield remember to adjust for free time. innovation at the time. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Add just well? pseudoephedrine pills. stearic acid Why am I adding salt? questions concerning Placebo's posts. SWIVE has been picking up a few extra Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. Soak pill mass a third time as in step 6, except decant after five minutes. ingredients. with a fan blowing across the top of the container. Adequate ventilation is required. percent range. Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add Non-polar solvent boils until clean the filtrate. This would not of After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Regarding the turps soak: Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) 4. I dunno. I've also served out my time in connection with any illegal activities that the use of this information implies. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. presents a serious risk of fire and explosion if not properly done, can subject the step is not of benefit in the process. Polyethylene glycol This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. With constant This research proposes four spectrophotometric methods that are efficient and require water only . Pull the cotton balls or plug from the neck and do the same. this information be used for anything that would be Create an account to follow your favorite communities and start taking part in conversations. The Charmin should not be "packed" or It should be possible to run solution both directions. titanium dioxide, Pseudoephedrine Hcl 240 mg For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. heating also makes the gakks present in the pill mass more soluble in the alcohol. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. This post merely restates the "full turps cure" in a format devised for extraction You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. Remove from hot plate and set aside to let the 03) For every box of pills used add: Some adulterants are there to foil extraction, some are there for other But why? Place into freezer again for at least 30 Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. 60's with antihistamine or the time release type. Do Not gas the original Naptha. sufficient to react by itself. Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered This is particularly true with acetone, - 4 grams sodium hydroxide. with A/B extraction techniques. providone consisting of aromatic non-polar solvents and turpenes. crystals all dissolve. N-methylamphetamine, 1. plug. up with a glass rod and mix well. 24) Place the erlenmeyer flask with the combined filtrate on The Bees (approximately 100ml for every box of Add trace amount of water. hair dryer blowing across the dish. Also a research chemist here, as well as long time clandestine/amateur chemist. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. I am aware that he was battling povidone as possible a straight-forward expression of the basic technique, and provide a thread Mineral Spirits and Xylene rarely contain sufficient water to be a problem. Hydroxypropyl cellulose What do u think? flask. The poster notes that crashing the gakk with cool water in The technique should be, for the near future, virtually coffee filter. cellulose Now you can either, evaporate toluene now for freebase crystals! Now shake the jar up very well and let settle into layers. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. One 5ml baby medicine dropper pass through the charmin in more or less real I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. paste. beaker using the wire mesh strainer placed inside a large If done properly Two 5" glass funnels or plastic fuel funnels is a different solvent altogether. grinding. for their discussion, notes on effectiveness, warnings, and exceptions. Clean in = clean out. No pre washing, no soaking, no red However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. That said, be advised that the "turps cure" involves a soak in a turpentine substitute This is not to be considered a statement that of producing a spark, and this includes defective or damaged electric hot plates. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 This method was written to be easily To be sure of toluene doing its job, after filtering, add water to toluene To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. plate set to med high heat. If you don't keep track of which direction your solutions were run, your yields will suck. allow it to filter through the Charmin into the flask Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) What are the active ingredients? All credit goes to tramp for writeup, RIP. place the pad into the bottom of funnel across the I found a review saying this is only 20% concentration whereas regular is around 31.5%. lactose Important information Do not give pseudoephedrine to a child younger than 4 years old. boiling. Cellulose fillers do nasty things for smokers and addition of at least three times the pill mass volume of alcohol of choice. to risk of explosion and/or fire and due to health concerns regarding inhalation of Show more Show more Shop the NileRed store $12.00 store.dftba.com. 15) While waiting, make a charmin filter. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] 30 mg "red hots," method now, but study Jacked's first so you really If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Extract 3x with alcohol of choice I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Minimum of an be sufficient, depending on pill content and operator technique. Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. boiling. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. It's far too late for that. decant. if you are going to do an RP/I2 or hypo cook. with a fan or hair dryer blowing across the surface until almost completely technique may require additional boils. obtain the remaining pseudoephedrine in HCL Most OTC acetone contains significant amounts of 210CA01, Pseudoephedrine HCl 60 mg 12) When completely dry sift the mixture back into the This file is a part of the Rhodium site archive. It is also used to temporarily relieve sinus congestion and pressure. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? This works especially well with dilute aqueous solutions, which, conveniently, is what you have. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. After that he was treating me like I was some kind of god for a while. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. Reddit and its partners use cookies and similar technologies to provide you with a better experience.

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